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The cleaning method of Methyltris(methyl ethyl ketoxime) silane can be carried out according to the following steps, with specific operations adjusted based on actual application scenarios:
Reaction System PreparationIn a solution containing methyltris(methyl ethyl ketoxime) silane hydrochloride salt, add end-capping agent and water at a molar ratio of methyltris(methyl ethyl ketoxime) silane : end-capping agent : water = 1 : 0.5–10 : 100–1000.
Reaction Condition Control
Temperature: 10–100 °C (preferably 20–80 °C)
Time: 0.2–12 hours
Stirring: Maintain continuous stirring to ensure uniform reaction.
Post-treatment Steps
After the reaction is completed, cool the system to room temperature, then filter to remove residual methyltris(methyl ethyl ketoxime) silane, obtaining a clean aqueous solution of methyl ethyl ketoxime hydrochloride salt.
Prefer high-purity end-capping agents to improve cleaning efficiency.
For wastewater treatment, technologies such as membrane separation, concentration, or desalination can be applied for further purification.